STRUCTURAL PROPERTY COMPARISON OF NEW AND USED DIAMOND-LIKE CARBON/TITANIUM DOUBLE-LAYER FILMS

Authors

  • Wichai Kongsri Faculty of Science and Technology, Valaya Alongkorn Rajabhat University, Klong Luang, Pathumthani, Thailand.
  • Ekachai Chongsereecharoen Reaserch Network NANOTEC-SUT on Advanced Nanomaterials and Characterization, School of Physics, Institute of Science, Suranaree University of Technology, Nakhon Ratchasima, Thailand.
  • Thanun Chunjaemsri Reaserch Network NANOTEC-SUT on Advanced Nanomaterials and Characterization, School of Physics, Institute of Science, Suranaree University of Technology, Nakhon Ratchasima, Thailand.
  • Piyaporn Thangdee Reaserch Network NANOTEC-SUT on Advanced Nanomaterials and Characterization, School of Physics, Institute of Science, Suranaree University of Technology, Nakhon Ratchasima, Thailand.
  • Warintorn Chatarat Reaserch Network NANOTEC-SUT on Advanced Nanomaterials and Characterization, School of Physics, Institute of Science, Suranaree University of Technology, Nakhon Ratchasima, Thailand.
  • Chanan Euaruksakul Synchrotron Light Research Institute (Public Organization), Nakhon Ratchasima, Thailand.
  • Rattikorn Yimnirun Research Network of NANOTEC-VISTEC on Nanotechnology for Energy and School of Energy Science and Engineering, Vidyasirimedhi Institute of Science and Technology, Wangchan, Rayong, Thailand.
  • Saroj Rujirawat Synchrotron Light Research Institute (Public Organization), Nakhon Ratchasima, Thailand.

Keywords:

DLC films, NEXAFS, XPS, Raman spectroscopy

Abstract

Diamond-like carbon (DLC) based films are usually applied to devices as protective coating in devices demanding excellent mechanical properties in order to improve tribological performances. In this work, DLC/Ti double-layer thin films were deposited on a moving part of Heads Gimbal Assembly (HGA) tester and were put in the operation for 1000 h. Comparison of structural properties of the newly deposited and after full operation samples was investigated. Surface morphology was examined by scanning electron microscopy (SEM). X-ray photoelectron spectroscopy (XPS) was used for examining chemical composition of films. Moreover, the structural properties were studied by near edge X-ray absorption fine structure (NEXAFS) spectroscopy and Raman spectroscopy. The results show a good tribological performance of the film as there was no significant difference between the new and used sample.

References

Bewilogua, K.and Hofmann. D. (2014). History of diamond-like carbon films-from first experiments to worldwide applications. Surface and Coatings Technol., 242:214-225

Robertson, J. (2002). Diamond-like amorphous carbon. Mater. Sci. Eng., 37 (4-6):129-281.

Wang, P., Wang, X., Xu, T., Liu, W., and Zhang, J. (2007). Comparing internal stress in diamond-like carbon films with different structure. Thin Solid Films., 515:6899-6903.

Park, C., Lee, J., and Park, Y.S. (2015). Thickness effects of TiC interlayer on tribological properties of diamond-like carbon prepared by unbalanced magnetron sputtering method. J. Nanoscience and Nanotechnology., 15:9009-9013.

Segura-Giraldo, B., Restrepo-Parra, E., and Arango-Arango, P.J. (2009). On the influence of a TiN interlayer on DLC coatings produced by pulsed vacuumarc discharge: compositional and morphological study. Applied Surface Scien., 256:136-141.

Thanun Chunjaemsri, Narong Chanlek, Usa Sukkha, Hideki Nakajima, Saroj Rujirawat, Rattikorn Yimnirun, and Pinit Kidkhunthod. (2020). Synchrotron-based NEXAFS analysis of thermal-treated diamond-like carbon films. Radiation Phy. and Chem., 175:108271.

Zhou, X., Tunmee, S., Suzuki, T., Phothongkam, P., Kanda, K., and Komatsu, K. (2017). Quantitative NEXAFS and solid-state NMR studies of sp3/(sp2+sp3) ratio in the hydrogenated DLC films. Diam. Relat. Mater., 73:232-240.

Watts, B., Thomsen, L., Dastoor, P.C. (2006). Methods in carbon K-edge NEXAFS: experiment and analysis. J. Electron. Spectrosc. Relat., 151(2):105-120.

Chunjaemsri, T., Chongsereecharoen, E., Chanlek, N., Kidkhunthod, P., Nakajima, H., Tunmee, S., Yimnirun, R., and Rujirawat, S. (2020). Influence of RF power and CH4 flow rate on properties of diamond-like carbon films deposited by PECVD technique. Radiation Phy. and Chem., 176:109073.

Ferrari, A.C. and Robertson, J. (2000). Interpretation of Raman spectra of disordered and amorphous carbon. Phys. Rev. B., 61(20):14095.

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Published

2026-08-28

How to Cite

Kongsri, W., Chongsereecharoen, E., Chunjaemsri, T., Thangdee, P., Chatarat, W., Euaruksakul, C., Yimnirun, R., & Rujirawat, S. (2026). STRUCTURAL PROPERTY COMPARISON OF NEW AND USED DIAMOND-LIKE CARBON/TITANIUM DOUBLE-LAYER FILMS. Suranaree Journal of Science and Technology, 29(2), 010115(1–4). retrieved from https://ph04.tci-thaijo.org/index.php/SUJST/article/view/15085

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Research Article