EFFECTS OF TITANIUM AND NIOBIUM ON MICROSTRUCTURE AND MECHANICAL ADHESION OF THERMAL OXIDE SCALES ON HOT-ROLLED LOW CARBON STEEL

Authors

  • Songkran Vongsilathai Department of Materials and Production Technology Engineering, Faculty of Engineering, King Mongkut’s University of Technology North Bangkok, Bangkok, Thailand.
  • Pakaipak Thapanathitikul Department of Materials and Production Technology Engineering, Faculty of Engineering, King Mongkut’s University of Technology North Bangkok, Bangkok, Thailand.
  • Komsan Ngamkham Department of Mechanical Engineering (Industrial Education), Faculty of Industrial Education, Rajamangala University of Technology Suvarnabhumi, Suphanburi, Thailand.
  • Tanaporn Rojhirunsakool Department of Materials and Production Technology Engineering, Faculty of Engineering, King Mongkut’s University of Technology North Bangkok, Bangkok, Thailand.

Keywords:

Ti addition, Nb addition, microalloyed steel, thermal oxide scale

Abstract

Improvement in strengthening steel without losing its ductility is the main development in the steel industry. The presence of a small amount of Ti and Nb concentrations significantly increases the strength of hot-rolled low carbon steel. In order to attain the finishing temperature of the hot-rolling process, the alloys are processed under 900°C in 17.2% steam mixed with an oxygen atmosphere and pure oxygen atmosphere for 1 min and 5 mins, respectively. The small amount of Ti/Nb additions influences the grain size and scale adhesion. The grain size was reduced by 16% in the Ti/Nb addition sample resulting in better strength properties by means of grain refinement. The Ti/Nb addition sample is less sensitive to the water vapour content than the base metal in an oxidizing atmosphere. The oxide scale in the Ti/Nb sample was found to have a Ti-doped magnetite phase. In both oxidizing atmospheres, the Ti/Nb addition sample showed lower strain initiating at the first spallation than that of the base metal sample, resulting in a weaker oxide scale adhesion.

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Published

2026-08-28

How to Cite

Vongsilathai, S., Thapanathitikul, P., Ngamkham, K., & Rojhirunsakool, T. (2026). EFFECTS OF TITANIUM AND NIOBIUM ON MICROSTRUCTURE AND MECHANICAL ADHESION OF THERMAL OXIDE SCALES ON HOT-ROLLED LOW CARBON STEEL. Suranaree Journal of Science and Technology, 26(1), 84–92. retrieved from https://ph04.tci-thaijo.org/index.php/SUJST/article/view/14636

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Research Article