PREPARATION AND PROPERTIES OF POROUS ALUMINA CERAMIC PRODUCED BY AN EXTRUSION PROCESS

Authors

  • Thanakorn Wasanapiarnpong Research Unit of Advanced Ceramics, Department of Materials Science, Faculty of Science, Chulalongkorn University, Bangkok, 10330, Thailand.
  • Yolnapa Ngoenngam Center of Excellence on Petrochemical and Materials Technology, Chulalongkorn University, Bangkok, 10330, Thailand.
  • Charusporn Mongkolkachit National Metal and Materials Technology Center, KlongLuang, Phathumthani, 12120, Thailand.
  • Suda Wanakitti National Metal and Materials Technology Center, KlongLuang, Phathumthani, 12120, Thailand.

Keywords:

Alumina, titania, porous ceramic, extrusion

Abstract

Porous alumina ceramic was fabricated by an extrusion method with the addition of titania as a sintering additive up to 20 wt%. Alumina powders were mixed and kneaded with titania and organic additives including binder (carboxy methyl cellulose, 7 wt% based on dry weight of alumina and titania; all wt% mentioned in this study based on the amount of inorganic powders excluding water), co-binder (polyvinyl alcohol, 1 wt%), plasticizer (polyethylene glycol, 0.5 wt%), lubricant (glycerin oil, 1 wt%), and solvent (water, 23 wt%). The resulting dough was extruded, dried at room temperature for 48 hours, and sintered at 1200oC for 1 hour in an electrical box furnace. The phasecomposition, microstructure, mechanical strength, and porosity of the sintered porous bodies were also investigated. With 5 and 10 wt% of TiO2, the bending strength of the sintered specimens ishigher than 18MPa with porosity of more than 40%.

References

Dong, Y., Chen, S., Zhang, X., Yang, J., Liu, X., and Meng, G. (2006). Fabrication and characterization of low cost tubular mineral-based ceramic membranes for micro-filtration from natural zeolite. J. Membr. Sci., 281(1-2):592-599.

Gosuphan, W. (2009). Fabrication and characterization of cordierite honeycomb ceramic from refractory industrial waste, [MSc. thesis]. Department of Materials Science, Faculty of Science, Chulalongkorn University, Bangkok, Thailand, 75p.

Isobe, T., Kameshima, Y., Nakajima, A., Okada, K., and Hotta, Y. (2006). Extrusion method using nylon 66 fibers for the preparation of porous alumina ceramics with oriented pores. J. Eur. Ceram. Soc., 26(12):2213-2217.

Isobe, T., Kameshima, Y., Nakajima, A., Okada, K., and Hotta, Y. (2007). Gas permeability and mechanical properties of porous alumina ceramics with unidirectionally aligned pores. J. Eur. Ceram. Soc., 27(1):53-59.

Isobe, T., Tomita, T., Kameshima, Y., Nakajima, A., and Okada, K. (2006). Preparation and properties of porous alumina ceramics with oriented cylindrical pores produced by an extrusion method. J. Eur. Ceram. Soc., 26(6):957-960.

Jedidi, I., Saïdi, S., Khmakem, S., Larbot, A., Elloumi-Ammar, N., Fourati, A., Charfi, A., and Ben Amar, R. (2009). New ceramic microfiltration membranes from mineral coal fly ash. Arabian J. Chem., 2(1):31-39.

Kritikaki, A. and Tsetsekou, A. (2009). Fabrication of porous alumina ceramics from powder mixtures with sol-gel derived nanometer alumina: Effect of mixing method. J. Eur. Ceram. Soc., 29(9):1603-1611.

Park, S.-Y., Jung, S.-W., and Chung, Y.-B. (2003). The effect of starting powder on the microstructure development of aluminaึaluminum titanate composites. Ceram. Int., 29(6):707-712.

Qi, H., Fan, Y., Xing, W., and Winnubst, L. (2010). Effect of TiO2 doping on the characteristics of macroporous Al2O3/TiO2 membrane supports. J. Eur. Ceram. Soc., 30(6):1317-1325.

Sathiyakumar, M. and Gnanam, F. D. (2003). Influence of additives on density, microstructure and mechanical properties of alumina. J. Mater. Process. Technol., 133(3):282-286.

Wang, Y., Zhang, Y., Liu, X., and Meng, G. (2007). Sol-coated preparation and characterization of macroporous -Al2O3 membrane support. J. Sol-Gel Sci. Technol.,41(3):267-275.

Downloads

Published

2026-08-28

How to Cite

Wasanapiarnpong, T., Ngoenngam, Y., Mongkolkachit, C., & Wanakitti, S. (2026). PREPARATION AND PROPERTIES OF POROUS ALUMINA CERAMIC PRODUCED BY AN EXTRUSION PROCESS. Suranaree Journal of Science and Technology, 21(1), 41–46. retrieved from https://ph04.tci-thaijo.org/index.php/SUJST/article/view/13926

Issue

Section

Research Article